It is one of the most widely used drugs that can lower fever and is used as a painkiller. The preparation of aspirin, the recrystallisation of aspirin and the melting point determination of aspirin. What does it mean when a sample has a higher melting point. Sep 17, 2019 your in text citations are just as important as your reference section. Fusion melting point data from nist standard reference database 69. Preparation of aspirin and determination of the melting point. Apr 07, 2015 purdue university online writing lab american psychological association apa style jordan. Electronic books, or ebooks, are digital versions of books that are meant to be read completely online. What is the purpose of apa formatting in college writing. Still it is common knowledge and i will not cite my source. These are the sources and citations used to research asprin. Or maybe youve just read the conference proceedings and want to cite them. The aspirin waste was discarded in the waste in the aspirin waste container.
Acetylsalicylic acid, european pharmacopoeia ep reference standard acetylsalicylic acid. Synthesis of aspirin and determination of melting point a. When there is no author move the title to the author spot. Purity can be determined by identify the melting point of aspirin. Dec 18, 2018 book with no author when a work has no author or editor, cite in the text the first few words of the reference list entry, usually the title and the year, and capitalise all major words. Aspirin melting point essay medicine and health articles. How to cite a book monograph in apa format nursing. Preparation and recrystallisation of aspirin contents page synopsis iii 1 introduction 1 1. A pure sample of a substance will melt at a sharply defined temperature, an impure sample will show a larger range. The problem with getting a value for the melting point of an organic substance is the purity of the material. Citation assistance industrial engineering research. The apa key elements page is a good place to start. Macroscale and microscale organic experiments book, 2003.
Apr 17, 2017 american psychological association, or apa, formatting is a system most commonly used to cite references in the social sciences. Find more information about crossref citation counts. Finally, the purity of the purified dry aspirin crystals can be determined by identifying the melting point while the amount of yield can be accounted for by weighing the aspirin sample after. Relatively pure white crystals of aspirin were obtained.
In the reference list, include a reference only for the jones book, which is the secondary source where you found your information. It is a physical book made of paper and cardstock or cardboard such as those on the library shelves. If you see an issue and serial numbers include them in parentheses, e. Page headers identify each page with the page number placed in the header at the right margin. Mar 12, 2020 a print book is one that can be held in your hands. Dec 23, 2019 is used in most literature, arts, and humanities courses. Pittsburgh pa section on practical pharmacy and dispensing, a. Use a running head at the left margin of the header if your instructor requires it or. This is a lab report on the synthesis of organic aspirin. Clicking on the donut icon will load a page at with additional details about the score and the social media presence for the given article. And in general, what should i do when i encounter contradicting chemical data. On the anomalous melting point and the decomposition of acetylsalicylic acid. Dec 23, 2019 for example, if you want to cite smiths idea, which you read about in jones book.
Use double quotation marks around the title of an article or chapter, and italicise the title of a periodical, book, brochure or report, both in the in text. This bibliography was generated on cite this for me on monday, august 24, 2015. To export a reference to this article please select a referencing style below. These are the sources and citations used to research aspirin bibliography. Books apa citation style subject guides at university of. The search on this page works by searching the content.
Also, your melting point range may be greater than 2 degrees. Melting point dictionary definition melting point defined. This book contains eight freestanding activities that can be used singly or as a coherent package in a wide range of teaching and learning situations for both. Chapters and parts of books american psychological association rules for formatting papers, intext citations, and end references. In college writing, the publication manual of the american psychological association is the predominant style guide used in the social sciences, business, economics and nursing. To prepare aspirin, salicylic acid is reacted with an excess of acetic anhydride. Synthesis and recrystallization of aspirin lab report uk essays. Bulletin of the chemical society of japan 1950, 23 1, 2325. Impurities in a solid lower the melting point, and also spread out the range make it broader 510 deg instead of 12, for example.
Melting point is the change from solid to liquid and is the same as freezing point. Apa style citation guide this handout is based on the 6th edition of the publication manual of the american psychological association apa, but is not a comprehensive guide. Follow title with publication date and publication information. The average values of the melting points obtained by the laboratories can therefore be used as constants for the substances in question, which have accordingly been established as who melting point reference substances and included in the who collection of authentic chemical substances. Abstract aspirin is the common name for the compound acetylsalicylic acid, widely used as a fever reducer and as a pain killer. Aspirin is a salicylate drug, often used as an analgesic to relieve minor aches and pains, as an antiinflammatory compound that inhibits cox1. A small amount of a strong acid is used as a catalyst which speeds up the reaction. A melting point capillary tube with 12cm depth of fine crystals was loaded. Either way, apa referencing has specific rules for citing a conference paper, so make sure you know how its supposed to. The apa 6 blog also provides information on how to use five levels of heading in an apa style paper as well as how to format each level of heading. How to format bibliographical entries for the cited reference page. The standard title for them in apa citation style is always references. This bibliography was generated on cite this for me on friday, july 21, 2017.
Nine years later however, the uspstf issued a grade b recommendation for. An example of melt is what you do to an ice cube when you put i. Reasons you might get a higher measured mp than the literature value include. Acetylsalicylic acid binds to and acetylates serine residues in cyclooxygenases, resulting in decreased synthesis of prostaglandin, platelet aggregation, and inflammation.
The reference page provides identifying information about the resources that were used in your paper. Chapter from an edited book with different authors for each chapter anthology berry, 2005. Because of this emphasis on the author of the work, most mla citation involves recording the authors name prominently in the intext citation with no mention of the date. This agent exhibits analgesic, antipyretic, and anticoagulant properties. Melting point is a useful measure for the purity of a solid. Meltingpoints dictionary definition meltingpoints defined. The ashford writing center provides many resources to help you follow correct citation style primarily apa and gives lessons and examples of how to paraphrase and cite sources. Aspirin or acetylsalicylic acid acetosal is a drug in the family of salicylates, often used as an analgesic against minor pains and aches, antipyretic against fever, and antiinflammatory. Do not italicize title if a journal article or book chapter. Oct 07, 2019 put edition and report numbers in parenthesis after book title. It is a derivative of salicylic acid which is also an. Examples based on the sixth edition of the publication manual from the apa.
At the end of the experiment, the result gotten should be a result of 40 60 % yield and a melting point that is around the theoretical melting point of aspirin, which is 5ac 6ac. Called aspirin and heart attacks, and the book had no author, you might cite the source as follows. Aspirin is used medically to reduce fever and pain. Preparation and recrystallisation of aspirin 1796 words 8 pages.
Miscellaneous the melting point of acetylsalicylic acid published by permission of the chairman of the committee of revision, u. Is the bibliography always called references in apa style. The concentration ratio of aspirin semenplasma was 0. Mar 01, 2007 the problem with getting a value for the melting point of an organic substance is the purity of the material. Create your citations, reference lists and bibliographies automatically using the apa, mla, chicago, or harvard referencing styles. The definition of melt is to turn from a solid to liquid as a result of exposure to heat. The crc handbook of chemistry and physics hbcp contains over 700 tables in over 450 documents which may be divided into several pages, all categorised into 17 major subject areas. Journal article citation help for apa, 6th edition. Reduce the sample to a fine powder by using mortar and pestle. Since you had such a low melting point range and also a very wide range the product acts like a substance that is very impure.
Citation machine helps students and professionals properly credit the information that they use. Premium american psychological association, apa style. Acs style guide 2006 edition addresses how to cite an msds. The synthesis of aspirin is classified as an esterification reaction. Apa format establishes a number of clear rules for how to cite works using author information. Apa prescribes specific structure, tone, format and citation requirements for academic and professional research and writing. The recrystallization and dissolution of acetylsalicylic acid ubc. After recrystallizing aspirin and drying the crystals 2 days, i ran a melting point on the sample and obtained a range of 2. Haynes 20 preparing aspirin by reacting salicylic acid and acetic anhydride, and recording its melting point was the aim of this experiment. Melting and boiling point the experiment melting point is approximately 5c. Hence, the depression of the melting point of individual crystals is related to the increased. Msds citation guide libguides at mississippi college.
Apr 17, 2009 in general will the melting point of an aspirin tablet be higher or lower than that of pure lab made aspirin powder. The specific format of your in text citations will vary depending upon the source and the number of authors to whom the source is attributed. Book with no author apa 6th edition university of lincoln. Capitalize the first word of a book title and the first word of the subtitle, if any, and any proper nouns. It was known that aspirin had some side effects that were caused by the level of acid in the aspirin itself, which made the stomach irate when ingested. I also used melting point determination to give further evidence towards the purity of aspirin.
In general will the melting point of an aspirin tablet be higher or lower than that of pure lab made aspirin powder. So youve been to an academic conference and you want to cite a presentation youve seen. Cite your chapter anthology in american psychological association 6th edition format for free. Aspirin, an acetyl derivative of salicylic acid, is a white, crystalline, weakly acidic substance, with a melting point of 6 c 277 f, and a boiling point of 140 c 284 f. Then, determine the melting point of aspirin using necessary apparatus. The apa citation style for books is simple and may be used to cite textbooks as well as encyclopedias and articles compiled in books. Aspirin is only found in individuals who have consumed this drug. Melting point apparatus is commonly used for this purpose. Bibliographic references are doublespaced and indented half an inch after the first line. For preparation of aspirin, acetic anhydride is added to the measured amount of salicylic acid.
Nist chemistry webbook the national institute of standards and technology nist uses its best efforts to deliver a high quality copy of the database and to verify that the data contained therein have been selected on the basis of sound scientific judgment. The melting point range of pure aspirin is 8140 c and the melting point range of the salicylic acid starting material is 158161 c. In chemistry, one of the most commonly used guides is the acs style guide published by. Put edition and report numbers in parenthesis after book title. Aspirin is an orally administered nonsteroidal antiinflammatory agent. Hoffman reduced the acid by mixing the aspirin with sodium salicylate, a extract found in the willow tree bark 1, which paved the way to todays most popular and inexpensive drug 2. The altmetric attention score is a quantitative measure of the attention that a research article has received online. Feb 01, 2018 proper bibliographic reference format.
The purity of sample was tested by determining its melting point range. Laboratory safety and waste disposal crystallization melting points, boiling points. Preparation and recrystallisation of aspirin writework. The citation can be easily removed later and until the paper is in its final version, you will know where to go back and verify the information. The narrow range of melting seems to indicate that the sample is pure, but the slightly depressed melting point doesnt support that. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. Write your reference entry as you would a normal journal article.
Results page 3 about sample apa synthesis free essays. Results page 7 about sample apa synthesis free essays. Mechanochemically synthesized nanomaterials for intermediate temperature solid oxide fuel cell membranes unpublished phd thesis. Theses apa referencing guide subject guides at murdoch. The freezing point for most substances increases with pressure. Thinlayer chromatography of pain killers teachers and technicians guide to the activities 1. Chapters and parts of books apa style guide libguides at. Results page 4 about sample apa synthesis free essays. This should help student learn, not just the specific format for different types of books, but also the pattern that apa uses to establish the correct citation. If the title is a book or webpage, italicize title and end with a period. If impurities are present in your crude sample, the melting point range for your product will be lower than the range of pure aspirin. Using thinlayer chromatography to investigate aspirin 7. In cold water aspirin is insoluble but as the water heats up the solute starts to dissolve.
The tale of seven remedies for a lean purse is the chapter title. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride. Due to its wide range, and lower value than that of the theoretical melting point of 6c, it was assessed that the prepared aspirin was impure. Apa format and style checklist general guidelines font style must be times new roman, arial, or courier new. Aspirin, also known as acetylsalicylic acid asa, is a medication used to reduce pain, fever. How to cite chemical literature chemistry research guides at.
Using recrystallisation improve the purity of aspirin biology. The aspirin crystals were observed under the microscope and were drawn on the result sheet. In apa format intext citation is a section that is used to credit history of the main writer in details. Chapters and parts of books apa style guide libguides. May 20, 2010 after recrystallizing aspirin and drying the crystals 2 days, i ran a melting point on the sample and obtained a range of 2. Mar 16, 20 by jordan pettigrew this tutorial gives a basic overview of how to cite sources using apa style. The mean peak concentration of salicylate in plasma was 49 microgramsml range, 4262 microgramsml, reached in. The amount of each compound should be the same because there is a 1. C, which is slightly lower than the literature range for aspirin of 46. To find out the purity of aspirin obtain by recrystallisation of prepared aspirin from reaction of salicylic acid with acetic anhydride. The experimental melting point range of aspirin was determined to be 122 2c. Preparation of aspirin experiment 5 introduction in this experiment you will prepare a sample of aspirin, recrystallize the raw product, and determine the percentage yield of the aspirin based on the limiting reactant.
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